问题 单项选择题

DOM is a platform and language- (51) API that allows programs and scripts to dynamically access and update the content, structure and style of WWW documents (currently, definitions for HTML and XML documents are part of the specification). The document can be further processed and the results of that processing can be incorporated back into the presented (52) . DOM is a (53) -based API to documents, which requires the whole document to be represented in (54) while processing it. A simpler alternative to DOM is the event-based SAX, which can be used to process very large (55) documents that do not fit info the memory available for processing.

A.text

B.image

C.page

D.graphic

答案

参考答案:C

实验题

阿司匹林(乙酰水杨酸)是由水杨酸和乙酸酐合成的

在生成乙酰水杨酸的同时,水杨酸分子间也能发生聚合反应,生成少量聚合物(副产物)。合成乙酰水杨酸的实验步骤如下:

① 向150mL干燥锥形瓶中加入2.0g水杨酸、5mL乙酸酐(密度1.08g/ml)和5滴浓硫酸,振荡,待其溶解后,控制温度在85~90℃条件下反应5~10min。然后冷却,即有乙酰水杨酸晶体析出。

② 减压过滤,用滤液淋洗锥形瓶,直至所有晶体被收集到布氏漏斗中。抽滤时用少量冷水洗涤晶体几次,继续抽滤,尽量将溶剂抽干。然后将粗产品转移至表面皿上,在空气中风干。

③ 将粗产品置于100mL烧杯中,搅拌并缓慢加入25mL饱和碳酸氢钠溶液,加完后继续搅拌2~3分钟,直到没有二氧化碳气体产生为止。过滤,用5~10mL蒸馏水洗涤沉淀,合并滤液于烧杯中,不断搅拌,慢慢加入15mL4mol/L盐酸,将烧杯置于冷水中冷却,即有晶体析出。抽滤,用冷水洗涤晶体1~2次,再抽干水分,即得产品(纯净物)1.9克。

请回答下列问题

(1)第①步中,要控制反应温度在85~90℃,应采用_________ 加热方法。用这种加热方法需要的玻璃仪器有__________________ 

(2)在第②步中,用冷水洗涤晶体,其目的是__________________ 

(3)第③步中,加入碳酸氢钠的作用是__________________ 加入盐酸的作用是__________________ 

(4)如何检验产品中是否混有水杨酸?___________________________

(5)试计算本次合成阿司匹林的产率为_________(保留二位有效数字)

单项选择题